Diesel fuel. I'd fill it full, by filling it through the shifter hole. Then put the tcase in neutral and run the tranny through the gears for a minute or two. That should circulate the diesel and break up any old oil. Then drain it (if the diesel comes out really contaminated, you flush it again), and refill with 80/90 gear oil.
I've used diesel to flush out a tcase that used to always get water in it.